By Kiyotaka Asakura; James J Spivey
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Rooney and H. Daly, Appl. , A, 2008, 340, 196. 72 S. I. Woo and C. G. Hill, J. Mol. , 1984, 24, 165. 73 B. C. Gates and H. ), Adv. , 2006, vol. 50, 2007, vol. 51, and 2009, vol. 52. 74 B. M. Weckhuysen, Chem. Soc. , 2010, 39, 4557, preface. 75 E. Stavitski and B. M. Weckhuysen, Chem. Soc. , 2010, 39, 4615. 76 I. E. Wachs, in ‘‘Handbook of Raman Spectroscopy’’ (I. R. ), Marcel Dekker, 2002. 77 M. A. Ban˜ares, I. E. Wachs, ‘‘Raman Spectroscopy of Catalysts’’, in Encyclopedia of Analytical Chemistry, John Wiley & Sons, 2010.
75 1C). 2 UV-vis-ED-XAFS-Raman Beale et al. described a cell to combine UV-Vis, laser Raman, and EDXAFS spectroscopy. A glass capillary held in a furnace holds the catalyst in powder form and the two optical spectroscopy techniques are coupled to the reactor via glass ﬁber, as illustrated in Fig. 12. 121 The design ensured that the same area on the catalyst was probed by the techniques. Fig. 12 Capillary reaction-spectroscopy cell for simultaneously measuring Raman/UV-vis (reﬂectance mode) and energy dispersive XAFS (transition mode).
2007, 51, 75. 82 E. Iglesia and A. T. Bell, J. Phys. , 2004, 108, 2345. 83 A. E. Lewandowska, M. A. Ban˜ares, D. F. Khabibulin and O. B. Lapina, J. Phys. Chem. C, 2009, 113, 20648. 84 M. Ruitenbeek, A. J. van dillen, F. M. F. de Groot, I. E. Wachs, J. W. Geus and D. C. Koningsberger, Top. , 2000, 10, 241. 85 H. Zhao, S. Bennici, J. Shen and A. Auroux, J. , 2010, 272, 176. 86 S. M. Bennici, B. M. Vogelarr, T. A. Nijhuis and B. M. Weckhuysen, Angew. Chem. Int. , 2007, 46, 5412. 87 G. Centi and S.